HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19699061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5-Fluoro-2-methylbenzoyl chloride | HCID 2737383 | — |
| Reactant | HCID 19438750 | HCID 19438750 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19699061 | HCID 19699061 | — |
Reaction Steps
As described for Example 1, a solution of 2 mmol of 5,6-dihydro-6-(4-aminobenzoyl)-4H-isoxazolo [5,4-d]thieno[3,2-b]azepine and 5 mmol of triethylamine is reacted with 2.2 mmol of 5-fluoro-2-methylbenzoyl chloride in 10 ml of dichloromethane under argon for 16 hours to give the product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532235 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-6124ab742d4f4f1ab1bbbd8900222073 |
| Source note | uspto-grants-1996_07 |