HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 9886271, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 10521963 | HCID 10521963 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 9886271 | HCID 9886271 | 90% |
Reaction Steps
The compound is prepared via the same procedure used to synthesize the compound of Example 8. Pure material is obtained by flash chromatography [hexane:EtOAc (50:50), EtOAc, CH2Cl2, 0.5-1% IPA in CH2Cl2 ] in 90% yield: mp 74°-76° C. 1H NMR (CDCl3) 0.96 (6H; t), 2.52 (4H; q), 2.88 (2H; t), 3.72 (2H; s), 3.82 (3H; s), 4.28 (2H; t), 6.70-6.80 (2H; m), 7.10 (1H; d), 7.62 (1H; d)ppm. MS m/z 383 (MH+). Anal (C21H26N4OS) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532263 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-24e313d9d82a4ea88b1250130ed98289 |
| Source note | uspto-grants-1996_07 |