HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalate → HCID 21471794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalate | HCID 71081 | — |
| Reactant | R-56109 hydrochloride | HCID 11334359 | — |
| Reactant | HCID 21471980 | HCID 21471980 | — |
| Product | HCID 21471794 | HCID 21471794 | 68.9% |
Reaction Steps
The reaction and procedure were conducted in a similar manner as in Example 24 using 0.7 g of 5-acetyl-2-(2-bromoethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine and 0.61 g of 4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidine hydrochloride to give 0.7 g of 5-acetyl-2-(2-(4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidin-1-yl)ethyl)-4,5,6,7-tetrahydrothieno[ 2,3-c]pyridine as an oil, m.p. 170°-172° C. as oxalate thereof.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532240 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-f88b1e03d19d447aae4d725e19b63a6a |
| Source note | uspto-grants-1996_07 |