HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(Bis(4-fluorophenyl)methylene)piperidine → 2-Methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(Bis(4-fluorophenyl)methylene)piperidine | HCID 2724436 | — |
| Edukt | 6-Acetyl-3-(2-chloroethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine | HCID 21471856 | — |
| Produkt | 2-Methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine | HCID 14423154 | — |
Reaktionsschritte
The reaction and procedure were conducted in a similar manner as in Example 24 using 0.7 g of 6-acetyl-3-(2-chloroethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine and 0.6 g of 4-(bis(4-fluorophenyl)-methylene)piperidine to give 0.5 g of 6-acetyl-3-(2-(4-bis(4-fluorophenyl)methylene)piperidin-1-yl)ethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine as an oil, m.p. 209°-211° C. as axalate thereof.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05532240 |
| Quelldatensatz | uspto-grants-1996_07 |
| ORD ID | ord-68b614ca92894a85b978322c3b4e2023 |
| Quellennotiz | uspto-grants-1996_07 |