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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1734050Erstellt: 25. Oktober 2026

4-(Bis(4-fluorophenyl)methylene)piperidine → 2-Methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine

https://huagongshe.com/reaction/1734050

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-(Bis(4-fluorophenyl)methylene)piperidineHCID 2724436—
Edukt6-Acetyl-3-(2-chloroethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridineHCID 21471856—
Produkt2-Methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridineHCID 14423154—

Reaktionsschritte

The reaction and procedure were conducted in a similar manner as in Example 24 using 0.7 g of 6-acetyl-3-(2-chloroethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine and 0.6 g of 4-(bis(4-fluorophenyl)-methylene)piperidine to give 0.5 g of 6-acetyl-3-(2-(4-bis(4-fluorophenyl)methylene)piperidin-1-yl)ethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine as an oil, m.p. 209°-211° C. as axalate thereof.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05532240
Quelldatensatzuspto-grants-1996_07
ORD IDord-68b614ca92894a85b978322c3b4e2023
Quellennotizuspto-grants-1996_07