HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalate → HCID 21472066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalate | HCID 71081 | — |
| Reactant | R-56109 hydrochloride | HCID 11334359 | — |
| Reactant | HCID 21471927 | HCID 21471927 | — |
| Product | HCID 21472066 | HCID 21472066 | — |
Reaction Steps
The reaction and procedure were conducted in a similar manner as in Example 24 using 2.0 g of 6-acetyl-(3-chloropropyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine and 2.0 g of 4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidine hydrochloride to give 0.5 g of 6-acetyl-3-(3-(4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidin-1-yl)propionyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine as an oil, m.p. 180°-182° C. as oxalate thereof.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532240 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-eacfd5e4f69c4cd4aa74c33a8eea5942 |
| Source note | uspto-grants-1996_07 |