HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl borate → HCID 19707206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl borate | HCID 8470 | — |
| Reactant | 3-Fluoro-5-(4-fluorophenoxy)phenyl bromide | HCID 19707210 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19707206 | HCID 19707206 | — |
Reaction Steps
This compound is prepared in a manner analogous to that of Step B of Example 6, using 9.1 grams (0.032 mole) of 3-fluoro-5-(4-fluorophenoxy)-phenyl bromide, 14 mL (0.035 mole) of n-butyllithium (2.5M in hexanes), and 10.4 mL (0.095 mole) of trimethyl borate in 100 mL of tetrahydrofuran, yielding 3-fluoro-5-(4-fluorophenoxy)phenylboronic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05532370 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-c7d16e85cdcf449fa96ab1efabff4384 |
| Source note | uspto-grants-1996_07 |