Propyl mercaptan → HCID 23293466, compound
Reaction equation
[S:1]([C:5]1[N:6]=[C:7]2[N:11]([C:12]=1C(OCC)=O)[CH:10]=[CH:9][S:8]2)([CH3:4])(=O)=O.[CH2:18](S)[CH2:19]C>>[CH2:4]([S:1][C:5]1[N:6]=[C:7]2[N:11]([CH:12]=1)[CH:10]=[CH:9][S:8]2)[CH2:18][CH3:19]Participants
3
Procedure
In a manner similar to the procedure in Reference Example 1, the oily title compound was prepared from ethyl 6-mesylimidazo[2,1-b]thiazole-5-carboxlate and n-propyl mercaptan. ##STR9## NMR(CDCl3)δ: 1.00(t, 3H), 1.43-1.90(m, 2H), 2.88(t, 2H), 6.83(d, 1H), 7.38(s, 1H), 7.47(s, 1H)
Sources & evidence
- ORD record
- ord-3cd826d7d6f84a1ead1855af3c7603cc
- Source dataset
- uspto-grants-1996_07
- Patent number
- US05534482
Reaction notes
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