HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86747977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 19612579 | HCID 19612579 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86747977 | HCID 86747977 | — |
Reaction Steps
A solution of methyl iodide (852 mg, 6.0 mmol) and 3-(3-(6,6,6-trifluorohexyloxy-1,2,5-thiadiazol-4-yl)-pyridine (630 mg, 2.0 mmol) in acetone (25 ml) was refluxed for 7 h. The solution was evaporated and the residue was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05534528 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-1df389b760db4968bb3fc0fa4547e78c |
| Source note | uspto-grants-1996_07 |