HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Alanine → HCID 86749624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Alanine | HCID 5950 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 88388405 | HCID 88388405 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86749624 | HCID 86749624 | 60.4% |
Reaction Steps
15.3 g 2,3,4-tribromothiophene carboxylic acid chloride in 60 ml dioxane are reacted in a manner analogous to Example 89 with 34.56 g L-alanine and 3.20 g NaOH in 60 ml H2O. After workup, 10.5 g (60.1% of theory) N-(2',3',4'-tribromothenoyl)-L-alanine with a melting point of 175°-179° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05534541 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-7bd422c00daa4e4b82db547f474421c8 |
| Source note | uspto-grants-1996_07 |