Dimethylamine → HCID 19438194, compound

HRID 1734714Notes

Reaction equation

[CH3:1][NH:2][CH3:3].[N:4]1[C:9](P(OC(C)C)(=O)OC(C)C)=[N:8][C:7]([P:20]([O:26][CH:27]([CH3:29])[CH3:28])(=[O:25])[O:21][CH:22]([CH3:24])[CH3:23])=[N:6][C:5]=1[P:30]([O:36][CH:37]([CH3:39])[CH3:38])(=[O:35])[O:31][CH:32]([CH3:34])[CH3:33]>>[CH3:1][N:2]([CH3:3])[C:9]1[N:8]=[C:7]([P:20]([O:26][CH:27]([CH3:28])[CH3:29])(=[O:25])[O:21][CH:22]([CH3:24])[CH3:23])[N:6]=[C:5]([P:30]([O:31][CH:32]([CH3:34])[CH3:33])(=[O:35])[O:36][CH:37]([CH3:39])[CH3:38])[N:4]=1

Participants

Reactant 2

HCID 674Dimethylamine

HCID 19438204HCID 19438204, compound

Product 1

HCID 19438194HCID 19438194, compound

Procedure

Following the procedure of Example 20, aqueous dimethylamine (40% w/w, 50.63 g, 20.25 g (CH3)2NH, 0.450 mol) was reacted with hexaisopropyl 1,3,5-triazine-2,4,6-triphosphonate (42.98 g) to produce tetraisopropyl 2-dimethylamino-1,3,5-triazine-4,6-diphosphonate.

Sources & evidence

ORD record: ord-5bfbab305d92434e918634ccca6f5747
Source dataset: uspto-grants-1996_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05534573

Reaction notes

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