Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | (5-Ethyl-2-oxo-1,3-dioxan-5-yl)methyl 2-methylprop-2-enoate | HCID 15340225 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 15340226 | HCID 15340226 | — |
Reaction Steps
11.4 g of 5-ethyl-5-methacryloyloxymethyl-2-oxo-1,3-dioxane, 3.2 g of methanol and 0.285 g of p-toluenesulfonic acid were dissolved in 100 g of 1,2-dichloroethane. The solution was stirred for 2 hours at 40° C. and evaporated in vacuo to remove the solvent. After removing white precipitates by filtration, the residue was further concentrated whereupon the title compound was recovered as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05534647 |
|---|
| Source dataset | uspto-grants-1996_07 |
|---|
| ORD ID | ord-212fb9b2def342a8a5ac3dba886a813d |
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| Source note | uspto-grants-1996_07 |
|---|
