HRID1734867

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)(C)c1ccc(C=O)cc1NC(=O)CC1c2ccccc2Oc2ccccc21

HCID19966116

未命名化合物

HCID178506592

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)c1ccc(C(O)CCCCCC2CCCCC2)cc1NC(=O)CC1c2ccccc2Oc2ccccc21

HCID19965982

未命名化合物

PROCEDURE

实验过程

Following a procedure similar to that described in Example 14, but using 5-cyclohexylpentylmagnesium iodide and N-(2-t-butyl-5-formylphenyl)-2-(9H-xanthen-9-yl)acetamide (prepared as described in Preparation 15) as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as a foam-like substance.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-045d75b895dd46feae573988f8729149
来源数据集: uspto-grants-1996_07
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05534529
来源说明: uspto-grants-1996_07

反应 SMILES

[CH:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][Mg]I)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:14]([C:18]1[CH:23]=[CH:22][C:21]([CH:24]=[O:25])=[CH:20][C:19]=1[NH:26][C:27](=[O:43])[CH2:28][CH:29]1[C:42]2[CH:41]=[CH:40][CH:39]=[CH:38][C:37]=2[O:36][C:35]2[C:30]1=[CH:31][CH:32]=[CH:33][CH:34]=2)([CH3:17])([CH3:16])[CH3:15]>>[C:14]([C:18]1[CH:23]=[CH:22][C:21]([CH:24]([OH:25])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH:1]2[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]2)=[CH:20][C:19]=1[NH:26][C:27](=[O:43])[CH2:28][CH:29]1[C:30]2[CH:31]=[CH:32][CH:33]=[CH:34][C:35]=2[O:36][C:37]2[C:42]1=[CH:41][CH:40]=[CH:39][CH:38]=2)([CH3:17])([CH3:15])[CH3:16]