HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 19068945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 7-Chloro-1-methyl-1,3-dihydro-2H-indol-2-one | HCID 14918454 | — |
| Product | HCID 19068945 | HCID 19068945 | 72% |
Reaction Steps
Prepared from POCl3 (17 ml), DMF (17 ml), (44) (7.5 g), yielding (47) 6.8 g (72%). M.p. 185°-187° C. In this reaction the reaction time was 48 h instead of 3 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05536721 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-d5991b8671c84595823f88db02b26bc3 |
| Source note | uspto-grants-1996_07 |