Potassium Hydroxide → HCID 19068986, compound

HRID 1735104Notes

Reaction equation

[OH-].[K+].[CH3:3][C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[N:9]([CH3:13])[C:8]1[S:14][C:15]([C:17]([O:19]C)=[O:18])=[CH:16][C:7]2=1>>[CH3:3][C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[N:9]([CH3:13])[C:8]1[S:14][C:15]([C:17]([OH:19])=[O:18])=[CH:16][C:7]2=1

Participants

Reactant 2

HCID 14797Potassium Hydroxide

HCID 19068934HCID 19068934, compound

Product 1

HCID 19068986HCID 19068986, compoundYield 100%

Procedure

Prepared from KOH (0.40 g), (52) (0.33 g) yielding (55) 0.312 g (100%). M.p. 216°-219° C.

Sources & evidence

ORD record: ord-182d27ef905f4b3d8fa8d8c6aadbc6f0
Source dataset: uspto-grants-1996_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05536721

Reaction notes

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