Potassium Hydroxide → HCID 19068955, compound

HRID 1735107Notes

Reaction equation

HRID 1735107 reaction equation
[OH-].[K+].[C:3]1([N:9]2[C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[C:11]3[CH:18]=[C:19]([C:21]([O:23]C)=[O:22])[S:20][C:10]2=3)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>>[C:3]1([N:9]2[C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[C:11]3[CH:18]=[C:19]([C:21]([OH:23])=[O:22])[S:20][C:10]2=3)[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 14797Potassium HydroxideHCID 849403HCID 849403, compound

Product 1

HCID 19068955HCID 19068955, compoundYield 94.3%

Procedure

Prepared from KOH (0.51 g), (51) (0.70 g) after reflux overnight yielding (58) 0.63 g (94%). M.p. 206°-207° C.

Workup

  1. temperatureafter reflux overnight

Sources & evidence

ORD record
ord-dd6e45d62399456889914a6e9c4adc9a
Source dataset
uspto-grants-1996_07
Patent number
US05536721

Reaction notes

Loading…