HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → (2,3-Dihydro-2,2-dimethylbenzofuran-7-ylmethyl)triphenylphosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 7-(bromomethyl)-2,2-dimethyl-3H-1-benzofuran | HCID 4271936 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | (2,3-Dihydro-2,2-dimethylbenzofuran-7-ylmethyl)triphenylphosphonium bromide | HCID 19705240 | — |
Reaction Steps
This compound is prepared in a manner analogous to that of Step A of Example 2, using 11.8 grams (0.049 mole) of 2,3-dihydro-2,2-dimethylbenzofuran-7-ylmethyl bromide and 13.0 grams (0.050 mole) of triphenylphosphine in about 100 mL of toluene, yielding (2,3-dihydro-2,2-dimethylbenzofuran-7-ylmethyl)triphenylphosphonium bromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05536725 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-724b722ef3904ea3b9eba66d14d68019 |
| Source note | uspto-grants-1996_07 |