Water → HCID 19705231, compound

HRID 1735332Notes

Reaction equation

HRID 1735332 reaction equation
[F:1][C:2]([F:21])([F:20])[C:3]1[CH:4]=[C:5]([CH:17]=[CH:18][CH:19]=1)[O:6][CH:7]1[CH2:16][CH2:15][C:10]2(OCC[O:11]2)[CH2:9][CH2:8]1.O>C(O)(=O)C>[F:1][C:2]([F:20])([F:21])[C:3]1[CH:4]=[C:5]([CH:17]=[CH:18][CH:19]=1)[O:6][CH:7]1[CH2:16][CH2:15][C:10](=[O:11])[CH2:9][CH2:8]1

Participants

4

Reactant 2

HCID 962WaterHCID 19705216HCID 19705216, compound

Product 1

HCID 19705231HCID 19705231, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

This compound was prepared in a manner analogous to that of Step D of Example 2, using 7.6 grams (0.025 mole) of 8-(3-trifluoromethylphenoxy)-1,4-dioxaspiro[4.5]decane and 25 mL of water in 50 mL of acetic acid, yielding 4-(3-trifluoromethylphenoxy)cyclohexanone.

Workup

  1. customThis compound was prepared in a manner analogous to that of Step D of Example 2

Sources & evidence

ORD record
ord-0444de5269574c7b84ada36f99ab2d3b
Source dataset
uspto-grants-1996_07
Patent number
US05536725

Reaction notes

Loading…