HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Bromo-2,2-dimethyl-2,3-dihydro-1-benzofuran → HCID 19705191, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Bromo-2,2-dimethyl-2,3-dihydro-1-benzofuran | HCID 219475 | — |
| Edukt | 1,4-Dioxaspiro[4.5]decan-8-one | HCID 567415 | — |
| Edukt | Magnesium | HCID 5462224 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | HCID 19705191 | HCID 19705191 | — |
Reaktionsschritte
This compound is prepared in a manner analogous to that of Step D of Example 7, using 9.2 grams (0.040 mole) of 5-bromo-2,3-dihydro-2,2-dimethylbenzofuran, 1.1 grams (0.044 mole) of magnesium turnings, and 6.2 grams (0.040 mole) of 1,4-cyclohexanedione mono-ethylene ketal in about 70 mL of tetrahydrofuran, yielding 1-(2,3-dihydro-2,2-dimethylbenzofuran-5-yl)-1-cyclohexen-4-one.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05536725 |
| Quelldatensatz | uspto-grants-1996_07 |
| ORD ID | ord-cbe5b1ca0c614db0bc921025e0e248c8 |
| Quellennotiz | uspto-grants-1996_07 |