HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Ethoxyphenyl)-2-(4'-difluoromethoxyphenyl)-ethene → 1-(4-Ethoxyphenyl)-2-(4'-difluoromethoxyphenyl)-ethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Ethoxyphenyl)-2-(4'-difluoromethoxyphenyl)-ethene | HCID 54057516 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-(4-Ethoxyphenyl)-2-(4'-difluoromethoxyphenyl)-ethane | HCID 19436101 | — |
Reaction Steps
19.7 g of 1-(4-ethoxyphenyl)-2-(4'-difluoromethoxyphenyl)-ethene are hydrogenated in 150 ml of THF analogously to Example 6ab), using 6 g of Pd/C (5% Pd) as catalyst. m.p.: 37° C., Δn=0.103, viscosity: 8
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05536442 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-42cc21c978df45ff97f42fc9ad42bdea |
| Source note | uspto-grants-1996_07 |