HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannane, tributylethyl- → methyl (E) 6-(1,3-dihydro-6-ethyl-7-methyl-3-oxo-4-p-toluenesulfonyloxyisobenzofuran-5-yl)-3,4-dimethyl-4-hexenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannane, tributylethyl- | HCID 88048 | — |
| Reactant | HCID 86748921 | HCID 86748921 | — |
| Product | methyl (E) 6-(1,3-dihydro-6-ethyl-7-methyl-3-oxo-4-p-toluenesulfonyloxyisobenzofuran-5-yl)-3,4-dimethyl-4-hexenoate | HCID 86748920 | — |
Reaction Steps
By following the procedure of part A and substituting vinyltributyltin with ethyltributyltin, and substituting methyl (E) 6-(1,3-dihydro-7-methyl-3-oxo-4-p-toluenesulfonyloxy-6-trifluoromethanesulfonyloxyisobenzofuran-5-yl)-4-methyl-4-hexenoate with methyl (E) 6-(1,3-dihydro-7-methyl-3-oxo-4-p-toluenesulfonyloxy-6-trifluoromethanesulfonyloxyisobenzofuran-5-yl)-3,4-dimethyl-4-hexenoate, there is obtained methyl (E) 6-(1,3-dihydro-6-ethyl-7-methyl-3-oxo-4-p-toluenesulfonyloxyisobenzofuran-5-yl)-3,4-dimethyl-4-hexenoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05536747 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-aa2aeb95925d4c9281f8a826509a1790 |
| Source note | uspto-grants-1996_07 |