化工社化工社 化学情報印刷レポート · 研究参考用
(4-Chlorophenyl)(phenyl)methanamine → N-(4-Chlorobenzhydryl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (4-Chlorophenyl)(phenyl)methanamine | HCID 409810 | — |
| 反応物 | S-2pyridyl 3-cyanoandrosta-3,5-diene-17beta-thiocarboxylate | HCID 15380265 | — |
| 生成物 | N-(4-Chlorobenzhydryl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide | HCID 15380276 | 70% |
反応手順
Following a procedure similar to that described in Example 3(b), but using S-2-pyridyl 3-cyanoandrosta-3,5 -diene-17β-thiocarboxylate [prepared as described in Example 3(a)] and 4-chlorobenzhydrylamine as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained in a yield of 70%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05536714 |
| 出典データセット | uspto-grants-1996_07 |
| ORD ID | ord-e4c2d681b9e84d62bd5ef220515465e1 |
| 出典メモ | uspto-grants-1996_07 |