HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → (8S,9S,10R,13S,14S,17S)-N-tert-butyl-10,13-dimethyl-3-oxo-1,2,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthrene-17-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | S-2-pyridyl 3-oxo-4-androstene-17beta-thiocarboxylate | HCID 15380261 | — |
| Product | (8S,9S,10R,13S,14S,17S)-N-tert-butyl-10,13-dimethyl-3-oxo-1,2,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthrene-17-carboxamide | HCID 475445 | — |
Reaction Steps
Following a procedure similar to that described in Example 2(b), but using 9.77 g of S-2-pyridyl 3-oxo-4-androstene-17β-thiocarboxylate [prepared as described in Example 2(a)] and 14 ml of t-butylamine, 8.9 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05536714 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-d42ffcfa68ef44b4af8ce1a72f9fd2c5 |
| Source note | uspto-grants-1996_07 |