HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → methyl (E)-2-bromomethyl-beta-methoxycinnamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | methyl (E)-beta-methoxy-2-methylcinnamate | HCID 86749647 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | methyl (E)-2-bromomethyl-beta-methoxycinnamate | HCID 11219857 | — |
Reaction Steps
200 g (0.97 mol) of methyl (E)-β-methoxy-2-methylcinnamate and 190 g (1.07 mol) of N-bromosuccinimide which has been washed with methanol and dried, in 2 l of dry tetrachloromethane, are irradiated with a 300 watt UV lamp for 75 min, during which the solution begins to reflux.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05538940 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-a8e06a4e78c94cf692b713ea53d48640 |
| Source note | uspto-grants-1996_07 |