HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfur Dioxide → HCID 19434129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfur Dioxide | HCID 1119 | — |
| Reactant | hydroxylamine-O-sulfonic acid | HCID 76284 | — |
| Reactant | HCID 19434051 | HCID 19434051 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 19434129 | HCID 19434129 | 72% |
Reaction Steps
A solution of the product from Step D (2.0 g, 6.19 mmol) was treated sequentially with n-butyllithium, sulfur dioxide and hydroxylamine-O-sulfonic acid in a manner essentially analogus to that described in Example 15, Step E to give an orange solid (1.78 g, 72%): mp 180°-182° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05538966 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-6a5213764e68404585706463aea15424 |
| Source note | uspto-grants-1996_07 |