HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19434849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19434969 | HCID 19434969 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19434849 | HCID 19434849 | 75.9% |
Reaction Steps
367 mg (0.818 mmol) of Compound 56 obtained in Example 56 was dissolved in 10 ml of ethanol, 1.23 ml of a 2N aqueous solution of sodium hydroxide was added and the mixture was stirred at room temperature for 17 hours. The precipitated crystals were collected by filtration to give 261 mg (69%) of Compound 57.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05539112 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-858e292daca64980ad5dd1898dc04999 |
| Source note | uspto-grants-1996_07 |