Sodium Tetrafluoroborate → HCID 22364564, compound

HRID 1736259Notes

Reaction equation

HRID 1736259 reaction equation
[Br-].[CH3:2][O:3][C:4]1[CH:18]=[CH:17][C:7]([C:8](=[O:16])[CH2:9][N+:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:6][CH:5]=1.[F:19][B-:20]([F:23])([F:22])[F:21].[Na+]>>[F:19][B-:20]([F:23])([F:22])[F:21].[CH3:2][O:3][C:4]1[CH:5]=[CH:6][C:7]([C:8](=[O:16])[CH2:9][N+:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 4343483Sodium TetrafluoroborateHCID 117093181-[2-(4-Methoxyphenyl)-2-oxoethyl]pyridin-1-ium bromide

Product 1

HCID 22364564HCID 22364564, compoundYield 85%

Procedure

The title compound was prepared similarly to Example 2 from 4-methoxyphenacylpyridinium bromide and sodium tetrafluoroborate in a yield of 85%.

Sources & evidence

ORD record
ord-67fff2bed73549c2b4f815639d88c63e
Source dataset
uspto-grants-1996_07
Patent number
US05541032

Reaction notes

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