HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Hydroxyphthalimide → HCID 54550453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Reactant | HCID 53939218 | HCID 53939218 | — |
| Product | HCID 54550453 | HCID 54550453 | 76% |
Reaction Steps
2',3'-Dideoxy-3'-C-styryladenosine underwent standard Mitsunobu reaction with N-hydroxyphthalimide to provide 2',3'-dideoxy-5'-O-phthalimido-3'-C-styryladenosine in 76% yield with a melting point of 145°-147° C. Anal.: C26H22N6O4.1/4 H2O Calcd.: C% 64.12; H% 4.65; N% 17.25; Found: C% 63.96; H% 4.58; N% 17.51.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05541307 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-193b877edbdc4cc7bb7772ff46018664 |
| Source note | uspto-grants-1996_07 |