Sodium borohydride → HCID 57100950, compound

Participants

Reaction Steps

180 mg (0.329 mmol) of (2R*,4S*)-2-benzyl-1-(2-pyridylacetyl)-N-(4-quinolylmethyl)-N-trifluoroacetyl-4-piperidinamine are reacted with 50 mg (1.32 mmol) of sodium borohydride in analogy to Example 2. The title compound ##STR44## is obtained as white foam. TLC: methylene chloride/methanol/conc. ammonia (700:50:1) Rf =0.28, FD-MS: M+ =450.

Provenance & Evidence