Sodium borohydride → HCID 54401466, compound

Participants

Reaction Steps

115 mg (0.200 mmol) of diastereomer B of (2R*,4S*)-2-benzyl-1-((S)-phenylalanyl)-N-(4-quinolylmethyl)-N-trifluoroacetyl-4-piperidinamine are reacted with 30 mg (0.801 mmol) of sodium borohydride in analogy to Example 2. The title compound ##STR54## is obtained as white foam. TLC: methylene chloride/methanol/conc. ammonia (700:50:1) Rf =0.20, FD-MS: M+ =478.

Provenance & Evidence