Sodium borohydride → HCID 44289257, compound

Participants

Reaction Steps

234 mg (0.440 mmol) of (2R*,4S*)-2-benzyl-1-benzoyl-N-(4-quinolylmethyl)-N-trifluoroacetyl-4-piperidinamine are reacted with 67 mg (1.76 mmol) of sodium borohydride in analogy to Example 2. The title compound ##STR61## is obtained as white foam. TLC: methylene chloride/methanol/conc. ammonia (700:50:1) Rf =0.33, FD-MS: M+ =435.

Provenance & Evidence