HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenethylamine, (-)- → HCID 21468665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenethylamine, (-)- | HCID 75818 | — |
| Reactant | Cyclohexanemethylamine | HCID 76688 | — |
| Reactant | 2-Bromo-N,N-dimethylacetamide | HCID 225544 | — |
| Reactant | 2-Bromo-1-(morpholin-4-yl)ethan-1-one | HCID 13996876 | — |
| Product | HCID 21468665 | HCID 21468665 | — |
Reaction Steps
By following the procedure of section (a) of this example but replacing (S)-1-phenylethylamine with twice the equivalent amount of (cyclohexylmethyl)amine and replacing 2-bromo-N,N-dimethylacetamide with an equivalent amount of 4-(2-bromo-1-oxoethyl)morpholine, 4-{2-[(cyclohexylmethyl)amino]-1-oxoethyl}morpholine [1H NMR(CDCl3) δ3.76-3.54 (m,3H), 3.43-3.33 (m,4H), 2.45 (d, J=6.6 Hz,2H), 2.41 (broad s,1H), 1.84-0.84 (m,11H)] was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05541163 |
| Source dataset | uspto-grants-1996_07 |
| ORD ID | ord-0804c8d9ba4542a3ac15c0d34101f35a |
| Source note | uspto-grants-1996_07 |