HRID1737125

反应详情

EQUATION

反应方程式

HRID 1737125 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.8 g (9.8 mmoles) of copper(II) acetate are dissolved in 100 ml of hot methanol and a solution of 1.5 g (20 mmoles) of glycine in 50 ml of methanol is added with stirring to the resulting solution. The solution turns cloudy under the effect of precipitated product. After stirring for 2 hours at a falling temperature, the product precipitated is filtered off and dried. Yield: 2.5 g (96% of the theoretical), Mp.:>210° C.

WORKUP

后处理

  1. stirringAfter stirring for 2 hours at a falling temperature
  2. customthe product precipitated
  3. filtrationis filtered off
  4. customdried