HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 178442700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 178516607 | HCID 178516607 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 178442700 | HCID 178442700 | — |
Reaction Steps
The aldehyde (8.46 mmol) was coupled to lawsone following the procedure set out in Example 42 using lawsone (1.18 g),THF (20 ml), pyrrolidine (672 μl), benzene (40 ml) and p-toluenesulphonic acid (1.95 g). 391 mg of the title compound was isolated after purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05962002 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-52acfb1f88a44f609e931ae1d08f361a |
| Source note | uspto-grants-1999_10 |