HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 57142402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 10051431 | HCID 10051431 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57142402 | HCID 57142402 | — |
Reaction Steps
The benzodiazepine of Example 17 (335 mg, 0.677 mmol) was treated with sodium borohydride in ethanol as described in Examples 12 and 13. The residue was chromatographed to afford the two title compounds (eluant EtOAc/Hexane 35:65 v/v).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05962451 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-a7e68d4593f44d3fa529011e9c5b400c |
| Source note | uspto-grants-1999_10 |