HCID 9932477, compound → HCID 9823268, compound

HRID 1737648Notes

Reaction equation

HRID 1737648 reaction equation
C[O:2][C:3]([C:5]1[S:6][CH:7]=[C:8]([CH3:29])[C:9]=1[N:10]([CH2:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1)[S:11]([C:14]1[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[CH:16][CH:15]=1)(=[O:13])=[O:12])=[O:4]>CCOCC>[CH2:22]([N:10]([S:11]([C:14]1[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[CH:16][CH:15]=1)(=[O:13])=[O:12])[C:9]1[C:8]([CH3:29])=[CH:7][S:6][C:5]=1[C:3]([OH:4])=[O:2])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 1

HCID 9932477HCID 9932477, compound

Product 1

HCID 9823268HCID 9823268, compoundYield 106%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

In the same manner as described in Example 11, 1.366 g (2.622 mmol) of the product of Example 8 provided 1.16 g (87%) of the desired carboxylic acid as a white solid after trituration with ether. Electrospray Mass Spec: 416 (M-H)-.

Sources & evidence

ORD record
ord-68ed5ce6bd9d410a97234a0d5b26d22c
Source dataset
uspto-grants-1999_10
Patent number
US05962481

Reaction notes

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