HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanal → HCID 21843576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanal | HCID 7707 | — |
| Reactant | 4-(1,2,4-Triazol-1-ylmethyl)benzonitrile | HCID 7537616 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 21843576 | HCID 21843576 | — |
Reaction Steps
1-[1-(4-cyanophenyl)-2-hydroxy-4-phenylbutyl]-1,2,4-triazole is prepared by the method described in Example 1 starting from 1-(4-cyanobenzyl)-1,2,4-triazole (2.0 g, 0.0108 mol), n-BuLi (0.0108 mol) and 3-phenylpropionaldehyde (1.74 g, 0.013 mol). The product is purified by flash chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05962495 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-5798cafc6a864229bbb0da743d3fc801 |
| Source note | uspto-grants-1999_10 |