HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium bisulfate → HCID 70276086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium bisulfate | HCID 516920 | — |
| Reactant | HCID 9836848 | HCID 9836848 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70276086 | HCID 70276086 | — |
Reaction Steps
1-[1-(4cyanophenyl)-3-(4-fluorophenyl)-3-hydroxypropyl]-1,2,4-triazole (100 mg) is heated with potassium hydrogen sulfate (400 mg) on oil bath at 140° C. for 2 hours. Methanol is added and the inorganic material is filtered off. Methanol is evaporated to give the product as a mixture of cis and trans isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05962495 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-7493e5dd83334a04a27691ab34952318 |
| Source note | uspto-grants-1999_10 |