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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1738091Generated: November 3, 2026

Methyl isothiocyanate → HCID 54517905, compound

https://huagongshe.com/reaction/1738091

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl isothiocyanateHCID 11167—
Reactant6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazoleHCID 22611560—
SolventDichloromethaneHCID 6344—
ProductHCID 54517905HCID 5451790548%

Reaction Steps

To a solution of 10.0 mg (0.0437 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole in 3.0 mL dichloromethane were added 6.2 mg (0.0874 mMol) methyl isothiocyanate. The reaction was mixed for 48 hours and to it were then added 0.15 gm (0.0874 mMol) aminomethylated polystyrene and the reaction mixed for an additional 18 hours. The reaction mixture was then filtered and the volatiles evaporated to give 6.3 mg (48%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05962473
Source datasetuspto-grants-1999_10
ORD IDord-302056a5c75c41819071f72d49f6555c
Source noteuspto-grants-1999_10