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2-Methyl-3-furoic acid → 6-(2-methylfur-3-oyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methyl-3-furoic acid | HCID 244756 | — |
| 反応物 | 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 22611560 | — |
| 生成物 | 6-(2-methylfur-3-oyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 22611530 | 99.1% |
反応手順
Beginning with 8.7 mg (0.038 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole and 11 mg (0.087 mMol) 2-methylfuran-3-carboxylic acid, 12.7 mg (99%) of the title compound were recovered as a beige solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05962473 |
| 出典データセット | uspto-grants-1999_10 |
| ORD ID | ord-dd2fa7ab9e48457eaef517124985d5de |
| 出典メモ | uspto-grants-1999_10 |