HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Furancarboxylic acid, 5-methyl- → 6-(5-methylfur-2-oyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Furancarboxylic acid, 5-methyl- | HCID 74710 | — |
| Reactant | 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 22611560 | — |
| Product | 6-(5-methylfur-2-oyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 22611408 | 53% |
Reaction Steps
Beginning with 8.7 mg (0.038 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole and 11.0 mg (0.084 mMol) 5-methylfuran-2-carboxylic acid, 6.8 mg (53%) of the title compound were recovered as a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05962473 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-6417349a56374788b11c76e007991999 |
| Source note | uspto-grants-1999_10 |