HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 131720940, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | HCID 7109657 | HCID 7109657 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131720940 | HCID 131720940 | — |
Reaction Steps
In 600 ml of MeOH were dissolved 60.00 g of Boc-Trp-NHNH2 and 21.00 g of benzaldehyde, and the mixture was stirred in the presence of 3.80 g of 10% palladium carbon for 18 hours in a hydrogen stream. Subsequent procedures were carried out in the same manner as in Reference example 21 to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965538 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-e4b2da1b0c2b47f2a576a794e349cab4 |
| Source note | uspto-grants-1999_10 |