HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-5-hydroxy-5-methyl-6-heptyne → 7-Ethoxymethyl-1-(5-hydroxy-5-methyl-6-heptynyl)-3-methylxanthine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-5-hydroxy-5-methyl-6-heptyne | HCID 13198054 | — |
| Reactant | 7-Ethoxymethyl-3-methylxanthine | HCID 13747684 | — |
| Product | 7-Ethoxymethyl-1-(5-hydroxy-5-methyl-6-heptynyl)-3-methylxanthine | HCID 21839351 | — |
Reaction Steps
44.84 g (0.2 mol) of 7-ethoxymethyl-3-methylxanthine were reacted with 32.13 g (0.2 mol) of 1-chloro-5-hydroxy-5-methyl-6-heptyne from Example 1B1), and worked up in analogy to Example 1B2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965555 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-e5a26538947f488996303ec8b03061a8 |
| Source note | uspto-grants-1999_10 |