HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromonaphthalene-2-sulfonyl chloride → HCID 22721859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromonaphthalene-2-sulfonyl chloride | HCID 14457741 | — |
| Reactant | HCID 22721924 | HCID 22721924 | — |
| Product | HCID 22721859 | HCID 22721859 | 20% |
Reaction Steps
Using an analogous procedure to that disclosed in Example 2, 1-(4-piperidinylcarbonyl)-4-(4-pyridyl)piperazine was reacted with 6-bromonaphth-2-ylsulphonyl chloride to give 1-[1-(6-bromonaphth-2-ylsulphonyl)piperidin-4-ylcarbonyl]-4-(4-pyridyl)piperazine in 20% yield, m.p. 229-230° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965559 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-948e872ad20042b4a5b481a707b00e53 |
| Source note | uspto-grants-1999_10 |