Thiazolidinedione → HCID 57186169, compound

HRID 1739028Notes

Reaction equation

HRID 1739028 reaction equation
[CH2:1]([O:8][C:9]1[C:18]([O:19][CH3:20])=[CH:17][C:12]([CH:13]=[CH:14][CH:15]=O)=[CH:11][C:10]=1[O:21][CH3:22])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:23]1[CH2:27][C:26](=[O:28])[NH:25][C:24]1=[O:29]>>[CH2:1]([O:8][C:9]1[C:18]([O:19][CH3:20])=[CH:17][C:12]([CH:13]=[CH:14][CH:15]=[C:27]2[S:23][C:24](=[O:29])[NH:25][C:26]2=[O:28])=[CH:11][C:10]=1[O:21][CH3:22])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 5437ThiazolidinedioneHCID 53982463HCID 53982463, compound

Product 1

HCID 57186169HCID 57186169, compoundYield 57%

Procedure

According to the same manner as that described in Example 1, 4-benzyloxy-3,5-dimethoxycinnamaldehyde was condensed with 2,4-thiazolidinedione to give 5-(4-benzyloxy-3,5-dimethoxycinnamylidene)-2,4-thiazolidinedione (yield: 57%). This product was recrystallized from chloroform-ethanol. Yellow prisms, mp: 217-218° C.

Sources & evidence

ORD record
ord-35fc3c939cb04192be05a733b7676516
Source dataset
uspto-grants-1999_10
Patent number
US05965589

Reaction notes

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