HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Isopropoxybenzaldehyde → HCID 11118803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Isopropoxybenzaldehyde | HCID 250077 | — |
| Reactant | Triethyl 4-phosphonocrotonate, mixture of isomers | HCID 5365783 | — |
| Product | HCID 11118803 | HCID 11118803 | 58% |
Reaction Steps
According to the same manner as that described in Reference Example 1, 4-isopropoxybenzaldehyde was reacted with triethyl 4-phosphonocrotonate to give ethyl (E,E)-5-(4-isopropoxyphenyl)pentadienoate as crystals (yield: 58%). The crystals were recrystallized from ether-hexane. Colorless prisms, mp: 64-65° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965589 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-6d46954ee70841059e05ab61887ed30b |
| Source note | uspto-grants-1999_10 |