HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminiumhydride → HCID 18546174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminiumhydride | HCID 21584524 | — |
| Reactant | HCID 86754595 | HCID 86754595 | — |
| Product | HCID 18546174 | HCID 18546174 | 63% |
Reaction Steps
According to the same manner as that described in reference Example 10, methyl (E)-3-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-butenoate was reduced with sobutyl aluminum hydride to give (E)-3-[4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-butenol (yield: 63%). This product was recrystallized from ethyl acetate-ether. colorless crystals, mp: 126-127° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965589 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-b6140d290cd6490f89298b0d2a3f32ab |
| Source note | uspto-grants-1999_10 |