HCID 10998484, compound → HCID 10954968, compound

HRID 1739037Notes

Reaction equation

HRID 1739037 reaction equation
[CH:1]([O:4][C:5]1[CH:10]=[CH:9][C:8](/[CH:11]=[CH:12]/[CH:13]=[CH:14]/[CH2:15][OH:16])=[CH:7][CH:6]=1)([CH3:3])[CH3:2]>[O-2].[O-2].[Mn+4]>[CH:1]([O:4][C:5]1[CH:6]=[CH:7][C:8](/[CH:11]=[CH:12]/[CH:13]=[CH:14]/[CH:15]=[O:16])=[CH:9][CH:10]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 10998484HCID 10998484, compound

Product 1

HCID 10954968HCID 10954968, compoundYield 99%

Reagents, catalysts & solvents 1

HCID 178418406HCID 178418406, compoundCatalyst

Procedure

According to the same manner as that described in Reference Example 20, (E,E)-5-(4-isopropoxyphenyl)-2,4-pentadienol was oxidized with activated manganese dioxide to give (E,E)-5-(4-isopropoxyphenyl)-2,4-pentadienal as an oil (yield: 99%).

Sources & evidence

ORD record
ord-c06d1ac8b4de4a549338736f76b9503c
Source dataset
uspto-grants-1999_10
Patent number
US05965589

Reaction notes

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