Thionyl Chloride → HCID 11098094, compound

HRID 1739039Notes

Reaction equation

HRID 1739039 reaction equation
O[CH:2]([CH2:8][CH2:9][C:10]1[CH:15]=[CH:14][C:13]([O:16][CH:17]([CH3:19])[CH3:18])=[CH:12][CH:11]=1)[C:3]([O:5][CH2:6][CH3:7])=[O:4].S(Cl)([Cl:22])=O>>[Cl:22][CH:2]([CH2:8][CH2:9][C:10]1[CH:15]=[CH:14][C:13]([O:16][CH:17]([CH3:19])[CH3:18])=[CH:12][CH:11]=1)[C:3]([O:5][CH2:6][CH3:7])=[O:4]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 10956460HCID 10956460, compound

Product 1

HCID 11098094HCID 11098094, compoundYield 27%

Procedure

According to the same manner as that described in Reference Example 34, ethyl 2-hydroxy-4-(4-isopropoxyphenyl)-butyrate was chlorinated with thionyl chloride to give ethyl 2-chloro-4-(4-isopropoxypheyl)butyrate as an oil (yield: 27%).

Sources & evidence

ORD record
ord-dd3bdb52494547968d6e58e4be42fa47
Source dataset
uspto-grants-1999_10
Patent number
US05965589

Reaction notes

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