反应详情

2.5 g of 4-octyloxybenzyl alcohol were dissolved in 20 ml of chloroform, and the resultant solution was further fed dropwise with 1.48 g of thionyl chloride and then stirred for 1 hour at room temperature. The solution reacted was poured into ice-water and extracted with chloroform. The organic layer resulted was then dried with anhydrous magnesium sulfate, and the solvent used was removed by distillation under reduced pressure, thereby affording 2.2 g of 4-octyloxybenzyl chloride.

1. customThe solution reacted
2. extractionextracted with chloroform
3. customThe organic layer resulted
4. dry with materialwas then dried with anhydrous magnesium sulfate
5. customthe solvent used was removed by distillation under reduced pressure