HCID 18944508, compound → HCID 18944502, compound

HRID 1739571Notes

Reaction equation

HRID 1739571 reaction equation
[CH:1]([N:4]([CH:29]([CH3:31])[CH3:30])[C:5]([C:7]1[CH:12]=[C:11]([N+:13]([O-:15])=[O:14])[C:10]([C:16]2[CH:21]=[CH:20][C:19]([C:22]([O:24]C)=[O:23])=[CH:18][CH:17]=2)=[C:9]([N+:26]([O-:28])=[O:27])[CH:8]=1)=[O:6])([CH3:3])[CH3:2]>C(OCC)(=O)C.C1CCCCC1>[CH:29]([N:4]([CH:1]([CH3:3])[CH3:2])[C:5]([C:7]1[CH:12]=[C:11]([N+:13]([O-:15])=[O:14])[C:10]([C:16]2[CH:17]=[CH:18][C:19]([C:22]([OH:24])=[O:23])=[CH:20][CH:21]=2)=[C:9]([N+:26]([O-:28])=[O:27])[CH:8]=1)=[O:6])([CH3:31])[CH3:30]

Participants

3

Reactant 1

HCID 18944508HCID 18944508, compound

Product 1

HCID 18944502HCID 18944502, compoundYield 103.4%

Reagents, catalysts & solvents 1

HCID 21867204Cyclohexane ethylacetateSolvent

Procedure

Using the procedure of Example 19, Stage C, 244.4 mg of product B prepared in Example 19, Stage B were reacted to obtain 244.5 mg of the expected product with a Rf=0.146 (cyclohexane/ethyl acetate 1/1).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-b3104c8a39994d37baef48a78bd105a2
Source dataset
uspto-grants-1999_10
Patent number
US05965763

Reaction notes

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